Modern Methods for Lipid AnalysiS by Liquid Chromatography/ mass spectrometry and Related Techniques

Resources for Lipid Analysis in the 21st Century

Table of contents

                                  Preface . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . iii

 

                                  Acknowledgments . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v

 

Chapter 1                Atmospheric Pressure Ionization Techniques in Modern

Lipid Analysis

William Craig Byrdwell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .             1

 

Chapter 2                Analysis of Phospholipids by Liquid Chromatography

Coupled with On-Line Electrospray Ionization Mass

Spectrometry and Tandem Mass Spectro m e t ry

Åsmund Larsen and Erlend Hvattum . . . . . . . . . . . . . . . . . . . . . .               19

 

Chapter 3                Electrospray Ionization with Low-Energy Collisionally

Activated Dissociation Tandem Mass Spectrometry of

Complex Lipids: Structural Characterization and

Mechanisms of Fragmentation

Fong-Fu Hsu and John Turk . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61

 

Chapter 4                Liquid Chromatography/Electrospray Ionization Mass

Spectrometry for Analysis of Oxidized Lipids

Arnis Kuksis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 179

 

Chapter 5                Analysis of Fatty Acids by APCI-MS

Tomá˘s ˘Rezanka and Jaroslav Votruba . . . . . . . . . . . . . . . . . . . . . 242

 

Chapter 6                Regiospecific Analysis of Triacylglycerols using High

Performance Liquid Chromatography/Atmospheric

Pressure Chemical Ionization Mass Spectrometry

Hazel R. Mottram . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .               276

 

Chapter 7                Qualitative and Quantitative Analysis of Triacylglycerols

by Atmospheric Pressure Ionization (APCI and ESI)

Mass Spectrometry Techniques

William Craig Byrdwell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .             298

 

Chapter 8                Analysis of Carotenoids Using Atmospheric Pressure

Chemical Ionization Mass Spectrometry

Natasa Pajkovic and Richard B. van Breemen . . . . . . . . . . . . . .                413

 

Chapter 9                Analysis of Molecular Species of Plant Glycolipids

by HPLC/APCI-MS

Ryo Yamauchi . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 431

 

Chapter 10              Liquid Chromatography/Mass Spectrometry Analysis of

Biosurfactant Glycolipids Secreted by Microorganisms

Alberto Nuñez, Robert A. Moreau, and Thomas A. Foglia . . . . .                447

 

Chapter 11              Analysis of Steroids by Liquid Chromatography—

Atmospheric Pressure Photoionization Mass Spectrometry

Risto Kostiainen and Tiina Kauppila . . . . . . . . . . . . . . . . . . . . . .               472

 

Chapter 12              Toward Total Cellular Lipidome Analysis by ESI Mass

Spectrometry from a Crude Lipid Extract

Xianlin Han and Richard W. Gross . . . . . . . . . . . . . . . . . . . . . . .               488

 

Chapter 13              Dual Parallel Liquid Chromatography/Mass Spectrometry

for Lipid Analysis

William Craig Byrdwell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .             510

 

Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .       577